[화학공학] 아닐린 합성(Synthesis of aniline) 실험(영문)
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- 2011.09.06 / 2019.12.24
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추천 연관자료
- 목차
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Ⅰ. Purpose
Ⅱ. Introduction & Background
Ⅲ. Apparatus
Ⅳ. Reagents
Ⅴ. Experimental process & notice
VI. Applied fields & References
- 본문내용
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The reaction occurs just with 1/20~1/60 of HCl
requirements in the reaction formula.
3-neck flask
The flasks are often long neck; sometimes they have the incision on the neck, which precisely defines the volume of flask.
They can be used in distillations, or in the heating a product.
These types of flask are alternatively called Florence flasks.
Liebig condenser
the most basic water-cooled design
It is much more efficient than a simple retort due to its use for liquid cooling
a Liebig condenser can condense a much greater flow of incoming vapour than an air condenser or retort
1.Place 18.3ml of nitrobenzene and add 25g of iron
powder in 3-neck flask with shaking.
2. Add the 6ml of hydrochloric acid slowly, as cooling
nitrobenzene using condenser. (Keep up 50~60℃)
- 참고문헌
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Book
Chemical Engineering Laboratory I
『최신유기합성실험』, 남기대 외2, 진영사 , p200~212
『Organic Chemistry』, 6th edition, John McMurry,
자유아카데미, p341,345
Internet
http://www.chemlocus.co.kr
www.sjparkk.com.ne.kr
http://stylist.textcube.com/
http://en.wikipedia.org/wiki/
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